词条 | 过程设计原理:合成、分析和评估 |
释义 | 图书信息出版社: 化学工业出版社; 第1版 (2002年8月1日) 外文书名: Process Design Principles Synthesis, Analysis, and Evaluation 平装: 824页 正文语种: 英语 开本: 16 ISBN: 9787502532703, 7502532706 条形码: 9787502532703 尺寸: 25.5 x 20.2 x 3.3 cm 重量: 1.3 Kg 作者简介作者:(美国)塞德(Sandler.W.D.) 内容简介在文件精神指导下,全国普通高等学校尤其是重点高校中兴起了使用国外教材开展教学活动的潮流。如生物技术与工程、环境科学与工程、材料科学与工程及作为其学科基础理论重要组成部分的化学技术和化学工程技术又是这股潮流中最为活跃的领域之一。在教育部“化工类专业人才培养方案及教学内容体系改革的研究与实践”项目组及“化工类专业创新人才培养模式、教学内容、教学方法和教学技术改革的研究与实践”项目组和“全国本科化学工程与工艺专业教学指导委员会”的指导和支持下,化学工业出版社及时启动了引进国外名校名著的教材工程。 目录Part one Process invention-heuristics and analysis 1.TheDesignProcess3 1.0Objectives3 1.1PrimitiveDesignProblems3 TypicalPrimitiveDesignProblem5 ProcessDesignTeam5 IndustrialConsultants5 1.2StepsinDesigningandRetrofittingChemical Processes6 AssessPrimitiveProblem6 SurveyLiterature8 ProcessCreation10 DevelopmentofBaseCase10 DetailedProcessSynthesisUsingAlgorithmic Methods11 PlantwideControllabilityAssessment11 DetailedDesign,EquipmentSizingandCost Estimation,ProfitabilityAnalysis,and Optimization12 WrittenProcessDesignReportandOral Presentation12 FinalDesign,Construction,Start-up,and Operation12 Summary13 1.3EnvironmentalProtection13 EnvironmentalIssues13 EnvironmentalFactorsinProcessDesign15 EnvironmentalDesignProblems18 1.4SafetyConsiderations19 SafetyIssues19 DesignApproachesTowardSafeChemical Plants22 1.5EngineeringEthics23 1.6RoleofComputers27 Spreadsheets28 MathematicalPackages28 ProcessSimulators28 ComputationalGuidelines30 1.7Summary30 References31 2.ProcessCreation32 2.0Objectives32 2.1Introduction32 2.2PreliminaryDatabaseCreation32 ThermophysicalPropertyData33 EnvironmentalandSafetyData37 ChemicalPrices37 Summary38 2.3Experiments38 2.4PreliminaryProcessSynthesis38 ContinuousorBatchProcessing39 ChemicalState41 ProcessOperations42 SynthesisSteps44 ExampleofProcessSynthesis:Manufactureof VinylChloride45 SynthesisTree56 Heuristics56 AlgorithmicMethods57 2.5DevelopmentoftheBase-CaseDesign57 DetailedProcessFlowsheet57 ProcessIntegration60 DetailedDatabase60 Pilot-PlantTesting61 ProcessSimulation62 2.6Summary62 References62 Exercises63 3.SimulationtoAssistinProcess Creation64 3.0Objectives64 3.1Introduction65 3.2PrinciplesofFlowsheetSimulation66 ProcessandSimulationFlowsheets66 UnitSubroutines77 CalculationOrder79 Recycle79 RecycleConvergenceMethods87 FlashwithRecycleProblem89 DegreesofFreedom90 ControlBlocksTDesignSpecifications91 FlashVesselControl94 BidirectionalInformationFlow(HYSYS)94 3.3SynthesisoftheTolueneHydrodealkylation Process98 ProcessSimulation101 3.4SimulationoftheMonochlorobenzene SeparationProcess104 UseofProcessSimulators105 3.5Summary106 References107 Exercises107 4.HeuristicsforProcessSynthesis112 4.0Objectives112 4.1Introduction113 4.2RawMaterialsandChemicalReactions114 4.3DistributionofChemicals116 InertSpecies117 PurgeStreams119 RecycletoExtinction122 Selectivity123 ReactiveSeparations125 4.4Separations126 4.5HeatRemovalfromandAdditionto Reactors128 HeatRemovalfromExothermic Reactors128 HeatAdditiontoEndothermicReactors131 4.6PumpingandCompression132 4.7Summary134 References134 Exercises135 PartTwoDETAILEDPROCESSSYNTHESIS-ALGORITHMICMETHODS 5.SynthesisofSeparationTrains141 5.0Objectives141 5.1Introduction141 5.2CriteriaforSelectionofSeparation Methods145 5.3SelectionofEquipment148 5.4SequencingofOrdinaryDistillation Columns150 5.5SequencingofGeneralVapor-Liquid SeparationProcesses156 5.6SequencingofAzeotropicDistillation Columns170 AzeotropyandPolyazeotropy170 ResidueCurves175 DistillationTowers178 SeparationTrainSynthesis188 5.7SeparationSystemsforGasMixtures194 MembraneSeparationbyGas Permeation197 Adsorption197 Absorption198 PartialCondensationandCryogenic Distillation199 5.8SeparationSequencingforSolid-Fluid Systems199 5.9Summary201 References201 Exercises202 6.SecondLawAnalysis207 6.0Objectives207 6.1Introduction207 6.2TheSystemandtheSurroundings210 6.3EnergyTransfer212 6.4ThermodynamicProperties213 6.5EquationsforSecondLawAnalysis215 6.6ExamplesofLost-WorkCalculations219 6.7ThermodynamicEfficiency222 6.8CausesofLostWork223 6.9ThreeExamplesofSecondLaw Analysis224 6.10Summary237 References237 Exercises238 7.HeatandPowerIntegration243 7.0Objectives243 7.1Introduction244 HeatIntegrationSoftware247 7.2MinimizingUtilitiesinHeatIntegration247 Temperature-IntervalMethod248 UsingGraphicalDisplays251 LinearProgrammingMethod254 7.3StreamMatchingatMinimumUtilities256 StreamMatchingatthePinch256 StreamMatchingUsingaMixed-Integer LinearProgram263 7.4MinimumNumberofHeat Exchangers--BreakingHeatLoops267 7.5OptimumApproachTemperature271 7.6SuperstructuresforMinimizationof AnnualizedCost274 7.7Heat-IntegratedDistillationTrains279 EffectofPressureonHeatIntegration279 Multiple-EffectDistillation281 HeatPumping,VaporReeompression,and ReboilerFlashing284 SuperstructuresforMinimizationof AnnualizedCost284 7.8HeatEnginesandHeatPumps286 PositioningHeatEnginesandHeat Pumps289 OptimalDesign292 7.9Summary295 References295 Exercises296 Partthree detailed design,equipment sizing,economics ,and optimization 8.HeatExchangerDesign303 8.0Objectives303 8.1Introduction303 HeatDuty303 HeatTransferMedia305 Temperature-DrivingForceforHeat Transfer308 PressureDrop312 8.2EquipmentforHeatExchange312 Double-PipeHeatExchangers312 Shell-and-TubeHeatExchangers314 Air-CooledHeatExchangers319 CompactHeatExchangers320 Temperature-DrivingForcesinShell-and- TubeHeatExchangers321 8.3HeatTransferCoefficientsandPressure Drop326 EstimationofOverallHeatTransfer Coefficients327 EstimationofIndividualHeatTransfer CoefficientsandFrictionalPressure Drop327 TurbulentFlowinStraight,SmoothDucts, Pipes,andTubesofCircularCross Section329 TurbulentFlowintheAnnularRegion BetweenStraight,Smooth,ConcentricPipes ofCircularCrossSection331 TurbulentFlowontheShellSideofShell-and- TubeHeatExchangers331 HeatTransferCoefficientsforLaminar-Flow, Condensation,Boiling,andCompactHeat Exchangers332 8.4DesignofShell-and-TubeHeat Exchangers333 8.5Summary335 References335 Exercises336 9.CapitalCostEstimation338 9.0Objectives338 9.1Introduction338 9.2CostCharts339 CostIndices342 InstallationCosts342 MaterialsandPressureConsiderations344 EquipmentSizes344 OtherInvestmentCosts345 LangFactorMethod348 9.3Equations348 HeatExchangers348 CylindricalProcessVessels349 Trays349 BlowersandCompressors349 9.4ASPENPLUS351 ProjectDates353 EquipmentLists353 EquipmentSizeandCostSpecifications356 RemainingInvestmentCosts361 CostIndices363 Results364 9.5DetailedCostEstimation368 9.6Summary369 References369 Exercises370 10.ProfitabilityAnalysis374 10.0Objectives374 10.1Introduction374 10.2CostSheet375 10.3TotalCapitalInvestmentandApproximate ProfitabilityMeasures378 WorkingCapital378 ApproximateProfitabilityMeasures378 10.4TimeValueofMoney384 CompoundInterest384 Annuities386 ComparisonofEquipmentPurchases388 10.5CashFlow391 Depreciation392 ProfitabilityMeasures393 NetPresentValue393 Investor'sRateofReturn394 10.6ASPENPLUS396 CostSheet396 WorkingCapital401 ProfitabilityMeasures401 Results404 10.7DetailedCostEstimation408 10.8Summary408 References409 Exercises409 11.OptimizationofProcessFlowsheets416 11.0Objectives416 11.1Introduction416 11.2NonlinearProgram417 ObjectiveFunction417 EqualityConstraints418 InequalityConstraints418 GeneralFormulation419 11.3OptimizationAlgorithm419 RepeatedSimulation421 InfeasiblePathApproach421 CompromiseApproach422 PracticalAspectsofFlowsheet Optimization422 11.4FlowsheetOptimizations--Case Studies423 11.5ASPENPLUS425 EnteringtheNLP425 AdjustingtheSimulationFlowsheet426 11.6Summary433 References433 Exercises433 PartFourPLANTWIDECONTROLLABILITYASSESSMENT 12.InteractionofProcessDesignandProcess Control439 12.0Objectives439 12.1Introduction439 12.2ControlSystemConfiguration444 ClassificationofProcessVariables444 Degrees-of-FreedomAnalysis446 12.3QualitativePlantwideControlSystem Synthesis449 12.4Summary454 References456 Exercises456 13.FlowsheetControllabilityAnalysis457 13.0Objectives457 13.1QuantitativeMeasuresforControllability andResiliency458 Relative-GainArray(RGA)459 DisturbanceCostandDisturbanceCondition Number467 13.2TowardAutomatedFlowsheetC&R Diagnosis471 Short-CutC&RDiagnosis471 GeneratingLow-OrderDynamic Models472 Tutorial:C&RAnalysisforHeat-Integrated DistillationColumns474 13.3CaseStudies480 13.4MATLABforC&RAnalysis493 13.5Summary496 References496 Exercises497 14.DynamicSimulationofProcess Flowsheets500 14.0Objectives500 14.1FundamentalConceptsinDynamic Simulation500 14.2DynamicSimulationUsingHYSYS501 14.3Control-LoopDefinition502 14.4ControllerTuningMethods504 On-LinePIControllerTuning504 Model-BasedPIControllerTuning505 14.5TutorialExercise:ControlofaBinary DistillationColumn509 14.6CaseStudies522 14.7Summary532 References532 Exercises532 PartFiveDESIGNREPORT15.WrittenProcessDesignReportandOral Presentation-537 15.0Objectives537 15.1WrittenReport538 SectionsoftheReport538 PreparationoftheWrittenReport543 PageFormat544 SampleDesignReports545 15.2OralDesignPresentation546 TypicalPresentation546 MediaforthePresentation546 RehearsingthePresentation547 WrittenHandout547 EvaluationoftheOralPresentation547 Videotapes549 15.3AwardCompetition549 15.4Summary549 References549 APPENDIXES I.ASPENPLUSinProcessDesign551 A-I.1ASPENPLUSInputForms551 A-I.2DrawinganASPENPLUSFlowsheet553 A-I.3ASPENPLUSParagraphs553 A-I.4NestedRecycleLoops554 A-I.5DesignSpecifications557 A-I.6InlineFORTRAN559 A-I.7CaseStudy:Monochlorobenzene SeparationProcess565 ASPENPLUSSimulationFlowsheetand Input565 InterpretationofProgramOutput565 II.HYSYSinProcessDesign581 A-II.1TheHYSYSModelingEnvironment581 A-II.2Steady-StateSimulation584 AcyclicProcesses584 ProcessesInvolvingRecycle605 Subflowsheets609 MultistageSeparationUsingtheColumn Subflowsheet609 Optimization618 A-II.3CaseStudy627 References629 I.PhaseEquilibriaandProcessUnit Models630 A-III.1PhaseEquilibria630 A-III.2FlashVessels630 A-III.3Pumps642 A-III.4CompressorsandExpanders644 A-III.5HeatExchangers646 HeatRequirementModels647 Shell-and-TubeHeatExchangers647 A-III.6ChemicalReactors651 StoichiometricReactorModels652 EquilibriumReactorModels654 KineticReactorModels655 A-III.7Separators666 Split-Fraction(BlackBox)Models667 Distillation:Fenske (Winn)-Underwood-GillilandShortcut Design667 Distillation:EdmisterApproximate GroupMethod672 Distillation:RigorousSimulationUsing theUnabridgedMESHEquations673 References679 IV.PhysicalPropertyEstimation,Solids Handling,andElectrolytes680 A-IV.1PhysicalPropertyEstimation680 DataBanks680 PropertyEstimation681 ASPENPLUS686 EstimatingParametersforPure Species690 SelectionofPropertyEstimationMethods andPropertyDataRegression692 A-IV.2NonconventionalComponentsand Substreams698 Substreams700 StreamClasses702 A-IV.3SolidsHandling703 A-IV.4Electrolytes709 ChemicalandPhaseEquilibrium709 ElectrolytesinProcessSimulators716 References720 V.ResidueCurvesforHeterogeneous Systems722 VI.SuccessiveQuadraticProgramming723 A-VI.1NLPandStationarityConditions723 A-VI.2SolutionoftheStationarity Equations724 References725 VII.GeneralAlgebraicModelingSystems (GAMS)726 A-VII.1InputFile727 Statements728 A-VII.2ExpandedFeatures:Documentation, VariableRedeclaration,and Display730 A-VII.3ExpandedFeatures:Sets,Tables, ParametersandScalars,andEquation Grouping734 A-VII.4Debugging737 References739 VIII.DesignProblemStatements740 A-VIII.0ContentsandIntroduction740 A-VIII.1Petrochemicals742 A-VIII.2PetroleumProducts748 A-VIII.3GasManufacture749 A-VIII.4Foods752 A-VIII.5Pharmaceuticals754 A-VIII.6Polymers755 A-VIII.7Environmental--AirQuality758 A-VIII.8Environmental--Water Treatment767 A-VIII.9Environmental--SoilTreatment771 A-VIII.10Environmental--Miscellaneous774 IX.DynamicSimulationUsing DYNAPLUS778 A-IX.1Introduction778 A-IX.2ProcedureforDynamicSimulation779 A-IX.3Control-LoopDefinitionin DYNAPLUS779 A-IX.4TutorialExercise:ControlofaBinary DistillationColumn780A-IX.5DynamicSimulationoftheMCB SeparationProcess791 X.HeuristicsforProcess,Equipment Design795 CompressorsandVacuumPumps795 ConveyorsforParticulateSolids796 CoolingTowers796 CrystallizationfromSolution797 Disintegration797 DistillationandGasAbsorption798 DriversandPowerRecoveryEquipment799 DryingofSolids799 Evaporators800 Extraction,Liquid-Liquid800 Filtration801 FluidizationofParticleswithGases801 HeatExchangers802 Insulation802 MixingandAgitation803 ParticleSizeEnlargement803 Piping804 Pumps804 Reactors804 Refrigeration805 SizeSeparationofParticles805 Utilities:CommonSpecifications806 Vessels(Drums)806 Vessels(Pressure)806 Vessels(StorageTanks)807 Xl.MaterialsofConstruction808 XILGenerationofLinearModelsin StandardForms810 AuthorIndex815 SubjectIndex817 |
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